The evaluation of microstructural-structural characteristics was conducted using microscopic, spectroscopic, and diffractometric methods. The nanocomposites were obtained in the combined process involving electrospinning of precursor nanofibers and catalytic chemical vapor deposition (CCVD) synthesis of carbon nanotubes directly on the surface of nanofibers. The aims of this work were analysis of the effect of the synthesis conditions on the microstructure, structure, and electrical properties of electrospun carbon nanofibers/disordered carbon nanotubes (eCNF/dCNT) nanocomposites, and analysis of the correlations between these properties. In particular, it enables Pawley refinement of powder diffraction data and size–strain analysis. It specializes in fitting a sum of bell-shaped functions to experimental data.
#FITTING BASLEINE WITH FITYK SOFTWARE#
Fityk is portable, open-source software for nonlinear curve fitting and data analysis. The journal is the primary place where crystallographic computer program information is published. Developments of instrumentation and crystallo-graphic apparatus, theory and interpretation, numerical analysis and other related sub-jects are also covered. Articles published in the Journal of Applied Crys-tallography focus on these methods and their use in identifying structural and diffusion-controlled phase transformations, structure–property relationships, structural changes of defects, interfaces and surfaces, etc. For further information see Many research topics in condensed matter research, materials science and the life sci-ences make use of crystallographic methods to study crystalline and non-crystalline mat-ter with neutrons, X-rays and electrons. Republication of this article or its storage in electronic databases other than as specified above is not permitted without prior permission in writing from the IUCr. Author(s) of this paper may load this reprint on their own web site or institutional repository provided that this cover page is retained.
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